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The existence of mixed-valence uranium ended up being investigated with a mixture of X-ray absorption near-edge structure and diffuse reflectance spectroscopy. Independent of the major hexavalent uranium, research for tetravalent uranium was also discovered, in line with the bond valence amount calculations. The successful preparation of UOF1 due to the fact very first pure uranium oxide hydrate framework sheds light on the architectural knowledge of the alteration of UO2
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