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This work focuses on the thermally induced variation in the nanostructure, size of primary particles and oxidative reactivity of diesel soot and a commercial carbon black in an inert gas environment at temperatures ranging from 600 to 1000 °C. Soot nanostructure and size were characterized by high-resolution transmission electron microscopy (HRTEM) and X-ray diffraction (XRD). The soot reactivity was evaluated with respect to activation energy (Ea) and characteristic oxidation temperature, including peak temperature (TP) and burnout tem