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Low limits of detection (i.e., 0.65 and 2.2 ng·mL-1) were obtained using the simplified sample preparation method. The recoveries were in the range 91-113.3 % with intra-day and inter-day precisions of ≤9.6 %. Further experimental results proved the method to be versatile for various hydrophilic toxins. A self-made microporous molecular sieve CS-Z1 has been found to have excellent adsorption performance for small molecular nitrile and pyridine pollutants in acrylonitrile production wastewater. In order to explore its adsorption mechanism,
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