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The separation of xylene isomers, especially p- and m-xylenes, is vital for the creation of numerous polymers and materials. However, existing advanced separation is situated upon fractional crystallisation at 220 K which is very power intensive. Here, we report the discrimination of xylene isomers via refinement for the pore dimensions in a number of permeable metal-organic frameworks, MFM-300, at sub-angstrom precision causing the suitable kinetic split of all of the three xylene isomers at room-te
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