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Besides Powder X-ray diffraction, Raman spectroscopy provided valuable informations first throughout the preliminary protonation action and 2nd by monitoring both the intercalation of liquid organic bases as well as the available acidity. N-alkylamines such as for example butylamine and octylamine had been discovered unsuitable to discriminate the layered solids while pyridine was more discerning. Pyridine didn't intercalate in H2W2O7, showcasing additionall
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