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Triethylamine (TEA), a typical kind of volatile organic compound, is widely used as an industrial solvent, which is a threat to environment and human health. In this paper, a novel In2O3 nanocube gas sensing material with high sensing performances was synthesized through a simple one-pot hydrothermal method. The gas sensing test results are satisfactory such that the single phase of In2O3 nanocubes even exhibits a quite higher response of 12-10 ppm of TEA at a lower temperature (180 °C) than many conventional In2O3-based complexes and main