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This analysis will discuss about a development of a Flow Injection Analysis-Atomic consumption Spectrometry (FIA-AAS) method that utilizes bentonite based useful product as a retention line. The split, preconcentration and trace evaluation regarding the Cr species within the liquid is effectively performed utilizing a Bt-MCCs mini-column in the FIA-AAS system. Analytical performance of the evolved method is called repeatability, linearity, and detection restriction. Analytical performance for Cr