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The new diamagnetic complex, [Zn2(N3)4(C6H6N2O)2] or [Zn2(pca)2(μ1,1-N3)2(N3)2] was synthesized using pyridine-2-carboxamide (pca) and azido ligands, and characterized using various techniques IR spectroscopy and single-crystal X-ray diffraction in the solid state, and nuclear magnetic resonance (NMR) in solution. The mol-ecule is placed on an inversion centre in space group P . The pca ligand chelates the metal centre via the pyridine N atom and the carbonyl O atom. One azido ligand bridges the two symmetry-related Zn2+ cations in the
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