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1-151.8% in GC-MS/MS analysis. The validated analysis systems were applied to biomonitoring of ten agricultural workers, and residues of 28 target pesticides were detected in their hair.Volatile Organic Compounds (VOCs) are a large group of chemicals mostly found in indoor environments such as homes and workplaces. Long term exposure to certain VOCs can cause symptoms in some individuals and therefore, monitoring and controlling air quality can help better manage chronic respiratory diseases. In this study, we aimed to develop an easy-to