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Lake sediment organic matter (OM) is composed of a variety of organic compounds differing in their biolability and origin. Sources of sediment OM can include terrestrial input from the watershed and algal/microbial metabolic byproducts residing in the water column or sediment. Dissolved organic phosphorus (DOP) is a critical component of OM in freshwater eutrophic lakes, often acting as a source for bioavailable phosphorus that fuels harmful algal and/or cyanobacterial blooms. Parallel extractions of lake sediment collected from Missisq