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In this work, submicron copper powder with narrow particle size distribution was synthesized via a simple methanol thermal reduction method without using any surfactants. Smaller copper powder with narrower particle size distribution could be realized by increasing the reaction temperature. Submicron copper powder with an average particle size of 206.6 nm and a particle size distribution of 100-300 nm could be obtained when the reaction temperature was 200 °C. Methyl formate was the only organic product found in the reaction. No organic
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